3H-1,2-Benzodithiol-3-one
- CAS: 1677-27-6
- Purity: 99%
- Chinese factory supply 3H-1,2-Benzodithiol-3-one 1677-27-6 in stock with high standard
Chinese factory supply 3H-1,2-Benzodithiol-3-one 1677-27-6 in stock with high standard
- Molecular Formula: C7H4 O S2
- Molecular Weight: 168.24
- Vapor Pressure: 0.000104mmHg at 25°C
-
Melting Point:
74-77 °C(lit.)
- Boiling Point: 337.6°Cat760mmHg
- Flash Point: 162.5°C
- PSA： 73.55000
- Density: 1.476g/cm3
- LogP: 2.32300
3H-1,2-Benzodithiol-3-one(Cas 1677-27-6) Usage
|
General Description |
3H-1,2-Benzodithiol-3-one is a heterocyclic building block. |
InChI:InChI=1/C7H4OS2/c8-7-5-3-1-2-4-6(5)9-10-7/h1-4H
1677-27-6 Relevant articles
Use of dimethyldioxirane for the oxidation of 1,2-dithiolan-3-ones to 1- oxides or 1,1-dioxides. Preparation of 3H-1,2-benzodithiol-3-one 1,1-dioxide (Beaucage sulfurizing reagent)
Marchan, Vicente,Gibert, Mariona,Messeguer, Angel,Pedroso, Enrique,Grandas, Anna
, p. 43 - 45 (1999)
Quantitative oxidation of 3H-1,2-benzodi...
1,2-Dithiolan-3-ones and derivatives structurally related to leinamycin. Synthesis and biological evaluation
Salvetti, Raul,Martinetti, Giovanni,Ubiali, Daniela,Pregnolato, Massimo,Pagani, Giuseppe
, p. 995 - 998 (2003)
Leinamycin, an antitumor antibiotic isol...
Understanding Reactivity and Assembly of Dichalcogenides: Structural, Electrostatic Potential, and Topological Analyses of 3 H-1,2-Benzodithiol-3-one and Selenium Analogs
Shukla, Rahul,Dhaka, Arun,Aubert, Emmanuel,Vijayakumar-Syamala, Vishnu,Jeannin, Olivier,Fourmigué, Marc,Espinosa, Enrique
, p. 7704 - 7725 (2020)
Molecular assembly and reactivity have b...
The automated synthesis of sulfur-containing oligodeoxyribonucleotides using 3H-1,2-benzodithiol-3-one 1,1-dioxide as a sulfur-transfer reagent
Iyer,Phillips,Egan,Regan,Beaucage
, p. 4693 - 4699 (1990)
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Reaction of n-propanethiol with 3H-1,2-benzodithiol-3-one 1-oxide and 5,5-dimethyl-1,2-dithiolan-3-one 1-oxide: Studies related to the reaction of antitumor antibiotic leinamycin with DNA
Behroozi,Kim,Gates
, p. 3964 - 3966 (1995)
We have studied the reaction of n-propan...
“Turn-on” fluorescent probe for detection of H2S and its applications in bioimaging
Zhao, Qi,Kang, Jin,Wen, Ying,Huo, Fangjun,Zhang, Yongbin,Yin, Caixia
, p. 8 - 12 (2018)
A novel fluorescent probe (named YQ-1) c...
Fluorescent probe for detecting hydrogen sulfide based on disulfide nucleophilic substitution-addition
Huo, Fangjun,Wang, Junping,Wu, Qing,Yin, Caixia
, (2020/05/08)
In view of the importance of hydrogen su...
Switchable Copper-Catalyzed Approach to Benzodithiole, Benzothiaselenole, and Dibenzodithiocine Skeletons
Huang, Meng-Qiao,K?rk?s, Markus D.,Li, Tuan-Jie,Liu, Jian-Quan,Shatskiy, Andrey,Wang, Xiang-Shan
supporting information, p. 3454 - 3459 (2020/04/30)
A copper-catalyzed reaction between 2-br...
Preparation method of benzodithiole skeleton compounds
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Paragraph 0029-0066, (2020/04/17)
The invention discloses a preparation me...
1677-27-6 Process route
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107-03-9
1-thiopropane
-
-
66304-00-5
1-oxo-1H-1λ4 -benzo[1,2]dithiol-3-one
-
-
1677-27-6
3H-1,2-benzodithiol-3-one
-
-
6028-61-1
dipropyl trisulfide
-
-
o-(Propyldithio)benzoic acid
-
-
629-19-6
Dipropyl disulfide
| Conditions | Yield |
|---|---|
|
With
triethylamine;
In
dichloromethane;
at 25 ℃;
for 2h;
Further byproducts given;
|
15%
29% |
-
-
107-03-9
1-thiopropane
-
-
66304-00-5
1-oxo-1H-1λ4 -benzo[1,2]dithiol-3-one
-
-
1677-27-6
3H-1,2-benzodithiol-3-one
-
-
52687-98-6
1,4-di(n-propyl)tetrasulfane
-
-
o-(Propyldithio)benzoic acid
-
-
629-19-6
Dipropyl disulfide
| Conditions | Yield |
|---|---|
|
With
triethylamine;
In
dichloromethane;
at 25 ℃;
for 2h;
Further byproducts given;
|
29%
15% |
1677-27-6 Upstream products
-
505-73-7
disulfanediyldiacetic acid
-
108085-49-0
2-carboxymethyldisulfanyl-benzoic acid
-
119-80-2
2,2'-dithiobenzoic acid
-
114062-91-8
2-acetyldisulfanyl-benzoic acid methyl ester
1677-27-6 Downstream products
-
7765-77-7
bis[2-(N-n-propylcarbamoyl)phenyl] disulfide
-
119-80-2
2,2'-dithiobenzoic acid
-
2527-63-1
2,2'-dithiobis(N-phenylbenzamide)
-
2527-58-4
2,2'-dithiobis(N-methylbenzamide)
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